Synthesis and characterization of 1,2-bis(2-(5-bromo-2-hydroxybenzilidenamino)-4-chlorophenoxy)ethane and its metal complexes: An experimental, theoretical, electrochemical, antioxidant and antibacterial study

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dc.authoridOkumus, Veysi/0000-0002-5505-2700
dc.authoridIlhan, Salih/0000-0003-0779-2744
dc.authoridBaykara, Haci/0000-0002-8319-0836
dc.authoridLevent, Abdulkadir/0000-0001-5792-419X
dc.contributor.authorIlhan, Salih
dc.contributor.authorBaykara, Haci
dc.contributor.authorOztomsuk, Abdussamet
dc.contributor.authorOkumus, Veysi
dc.contributor.authorLevent, Abdulkadir
dc.contributor.authorSeyitoglu, M. Salih
dc.contributor.authorOzdemir, Sadin
dc.date.accessioned2024-12-24T19:27:44Z
dc.date.available2024-12-24T19:27:44Z
dc.date.issued2014
dc.departmentSiirt Üniversitesi
dc.description.abstractA new Schiff base ligand was synthesized by reaction of 5-bromosalicylaldehyde with 1,2-bis(4-chloro-2-aminophenoxy)ethane. Then the Schiff base complexes were synthesized by the reaction of metal salts and the novel Schiff base. The molar conductivity properties of the complexes were studied and found out that the complexes are nonelectrolytes. The structures of the ligand and its metal complexes were characterized by elemental analysis, FT-IR, UV-VIS, magnetic susceptibility measurements, molar conductivity measurements, and thermal gravimetric analysis. In addition antioxidant, theoretical NMR studies and cyclic voltammetry of the complexes were done. Two methods namely metal chelating activity and diphenylpicrylhydrazyl (DPPH) radical scavenging method were used to determine the antioxidant activity, and antibacterial properties of the compounds were also studied. (C) 2013 Elsevier B.V. All rights reserved.
dc.description.sponsorshipScientific Research Projects Unit of Siirt University, (Turkey) [BAP-2011-SIUFED-YL1]
dc.description.sponsorshipThis study was supported by Scientific Research Projects Unit of Siirt University (Project code: BAP-2011-SIUFED-YL1), (Turkey).
dc.identifier.doi10.1016/j.saa.2013.08.069
dc.identifier.endpage642
dc.identifier.issn1386-1425
dc.identifier.issn1873-3557
dc.identifier.pmid24096058
dc.identifier.scopus2-s2.0-84884949144
dc.identifier.scopusqualityQ1
dc.identifier.startpage632
dc.identifier.urihttps://doi.org/10.1016/j.saa.2013.08.069
dc.identifier.urihttps://hdl.handle.net/20.500.12604/6766
dc.identifier.volume118
dc.identifier.wosWOS:000328005400085
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.language.isoen
dc.publisherPergamon-Elsevier Science Ltd
dc.relation.ispartofSpectrochimica Acta Part A-Molecular and Biomolecular Spectroscopy
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241222
dc.subjectSchiff base complexes
dc.subjectCyclic voltammetry
dc.subjectAntioxidant
dc.subjectGaussian
dc.subjectDFT
dc.subjectHF
dc.titleSynthesis and characterization of 1,2-bis(2-(5-bromo-2-hydroxybenzilidenamino)-4-chlorophenoxy)ethane and its metal complexes: An experimental, theoretical, electrochemical, antioxidant and antibacterial study
dc.typeArticle

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