A novel liquid-liquid extraction for the determination of naphthalene by GC-MS with deuterated anthracene as internal standard

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dc.authoridCHORMEY, DOTSE SELALI/0000-0002-7412-7800
dc.authoridERARPAT BODUR, Sezin/0000-0002-9879-6662
dc.authoridOzzeybek, Gozde/0000-0001-5817-1097
dc.contributor.authorErarpat, Sezin
dc.contributor.authorOzzeybek, Gozde
dc.contributor.authorChormey, Dotse Selali
dc.contributor.authorErulas, Fatih
dc.contributor.authorTurak, Fatma
dc.contributor.authorBakirdere, Sezgin
dc.date.accessioned2024-12-24T19:24:36Z
dc.date.available2024-12-24T19:24:36Z
dc.date.issued2017
dc.departmentSiirt Üniversitesi
dc.description.abstractPolycyclic aromatic hydrocarbons are known for their carcinogenic and mutagenic effects on human health. This therefore calls for the regulation of their concentrations in air, water, and soil. Naphthalene as the simplest in structure of the polycyclic aromatic hydrocarbons is mainly used as a starter material for other chemicals but also has impacts on human health. A method is therefore proposed for the determination of naphthalene in water samples by gas chromatography mass spectrometry after liquid-liquid extraction. The extraction method was optimized to improve the extraction output, thereby lowering the limit of detection. The limits of detection and quantification obtained for naphthalene were 4.4 and 14.6 ng mL(-1), respectively. Deuterated anthracene was used as internal standard to enhance the precision of the method, for which a relative standard deviation of 4.3% was obtained. The percent recovery of naphthalene obtained from tap water was ranged between 93.8 and 102.2.
dc.description.sponsorshipYildiz Technical University
dc.description.sponsorshipThe authors thank Yildiz Technical University for supporting this research.
dc.identifier.doi10.1007/s10661-017-6250-6
dc.identifier.issn0167-6369
dc.identifier.issn1573-2959
dc.identifier.issue10
dc.identifier.pmid28963642
dc.identifier.scopus2-s2.0-85030247763
dc.identifier.scopusqualityQ2
dc.identifier.urihttps://doi.org/10.1007/s10661-017-6250-6
dc.identifier.urihttps://hdl.handle.net/20.500.12604/6046
dc.identifier.volume189
dc.identifier.wosWOS:000413354400016
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofEnvironmental Monitoring and Assessment
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241222
dc.subjectLiquid-liquid extraction
dc.subjectNaphthalene
dc.subjectAnthracene D-10
dc.subjectGC-MS
dc.titleA novel liquid-liquid extraction for the determination of naphthalene by GC-MS with deuterated anthracene as internal standard
dc.typeArticle

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