Synthesis, characterization and experimental, theoretical, electrochemical, antioxidant and antibacterial study of a new schiff base and its complexes

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dc.authoridhttps://orcid.org/0000-0002-5505-2700en_US
dc.contributor.authorBaykara, Haci
dc.contributor.authorİlhan, Salih
dc.contributor.authorLevent, Abdulkadir
dc.contributor.authorSeyitoğlu, Salih
dc.contributor.authorÖzdemir, Sadin
dc.contributor.authorOkumuş, Veysi
dc.contributor.authorTomsuk, Abdussamet
dc.contributor.authorCornejo, Mauricio
dc.date.accessioned2019-12-25T11:24:51Z
dc.date.available2019-12-25T11:24:51Z
dc.date.issued2014en_US
dc.departmentFen - Edebiyat Fakültesien_US
dc.description.abstractA new Schiff base ligand was synthesized by reaction of salicylaldehyde with 1,6-bis(4-chloro-2-aminophenoxy) hexane. Then the Schiff base complexes were synthesized by metal salts and the Schiff base. The metal to ligand ratio of metal complexes was found to be 1:1. The Cu(II) complex is proposed to be square planar and the Co(II), Ni(II), Mn(II) and Zn(II) complexes are proposed to be tetrahedral geometry. The Ti(III) and V(III) complexes are proposed to be a capped octahedron in which a seventh ligand has been added to triangular face. The complexes are non-electrolytes as shown by their molar conductivities (KM). The structure of metal complexes is proposed from elemental analysis, FT-IR, UV–vis, magnetic susceptibility measurements, molar conductivity measurements, Mass Spectra and thermal gravimetric analysis. In addition antimicrobial and antioxidant studies, cyclic voltammetry of the complexes, theoretical 1H NMR and HOMO–LUMO energy calculations of the new di-functional ligand were done.en_US
dc.description.provenanceSubmitted by Veysi OKUMUŞ (veysiokumus@siirt.edu.tr) on 2019-12-23T17:04:34Z No. of bitstreams: 1 A20.pdf: 1788179 bytes, checksum: 7e7fa422058c2694f8a08123230753e2 (MD5)en
dc.description.provenanceApproved for entry into archive by Esra Diriarın (esradiriarin@siirt.edu.tr) on 2019-12-25T11:24:51Z (GMT) No. of bitstreams: 1 A20.pdf: 1788179 bytes, checksum: 7e7fa422058c2694f8a08123230753e2 (MD5)en
dc.description.provenanceMade available in DSpace on 2019-12-25T11:24:51Z (GMT). No. of bitstreams: 1 A20.pdf: 1788179 bytes, checksum: 7e7fa422058c2694f8a08123230753e2 (MD5) Previous issue date: 2014en
dc.identifier.citationBaykara, H., Ilhan, S., Levent, A., Seyitoglu, M. S., Özdemir, S., Okumuş, V., ... & Cornejo, M. (2014). Synthesis, characterization and experimental, theoretical, electrochemical, antioxidant and antibacterial study of a new Schiff base and its complexes. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 130, 270-279.en_US
dc.identifier.endpage279en_US
dc.identifier.pmid24792202
dc.identifier.scopus2-s2.0-84899674505
dc.identifier.scopusqualityQ1
dc.identifier.startpage270en_US
dc.identifier.urihttps://hdl.handle.net/20.500.12604/2420
dc.identifier.volume130en_US
dc.identifier.wosWOS:000338806800036
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.institutionauthorOkumuş, Veysi
dc.language.isoenen_US
dc.publisherSpectrochimica Acta Part A: Molecular and Biomolecular Spectroscopyen_US
dc.relation.ispartofSpectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.snmzKG_20241224
dc.subject1,6-Bis(4-chloro-2-aminophenoxy)hexaneen_US
dc.subjectCyclic voltammetryen_US
dc.subjectSalicyaldehydeen_US
dc.subjectBiological activitiesen_US
dc.subjectMass Spectra Gaussian 09 and HOMO–LUMOen_US
dc.titleSynthesis, characterization and experimental, theoretical, electrochemical, antioxidant and antibacterial study of a new schiff base and its complexesen_US
dc.typeArticleen_US

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