Metal chelate based site recognition of ceruloplasmin using molecularly imprinted polymer/cryogel system

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dc.authoridhttps://orcid.org/0000-0002-8014-7760en_US
dc.contributor.authorDolak, Ibrahim
dc.contributor.authorCanpolat, Gurbet
dc.contributor.authorErsöz, Arzu
dc.contributor.authorSay, Rıdvan
dc.date.accessioned2019-12-30T06:58:03Z
dc.date.available2019-12-30T06:58:03Z
dc.date.issued2020en_US
dc.departmentFen - Edebiyat Fakültesien_US
dc.description.abstractIn the present study, N-Acetylneuraminic acid (NANA)-imprinted poly(2-hydroxyethyl methacrylate- N-methacryloyl-(L)-histidin-Cu(II)) p(HEMA-(MAH)2-Cu(II)) has been synthesized by radical polymerization for site recognition of ceruloplasmin. Prepared imprinted cryogel has been characterized by scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR). When the binding capacity of NANA-imprinted cryogel (MIP) was compared with nonimprinted cryogel (NIP), it was found that MIP has higher adsorption capacity. The maximum amount of binding NANA has found as 83.20 mgg−1 at pH 7.0 with flow rate of 1 mLmin−1 at 25°C. Selectivity experiments for MIP and NIP cryogel have been carried out via the NANA/D-mannose and ceruloplasmin/immunoglobulin G (IgG) pair separately and the relative selectivity coefficient (k’) has found as 77.46 and 17.97, respectively. Applicable of the MIP in human serum has been studied and resulted successfully.en_US
dc.description.provenanceSubmitted by Gurbet Canpolat (gokalp.gurbet@siirt.edu.tr) on 2019-12-27T15:21:58Z No. of bitstreams: 1 Metal chelate based site recognition of ceruloplasmin using molecularly imprinted polymer cryogel system (1).pdf: 1574877 bytes, checksum: d539d9c226f04e149f22825f3419f412 (MD5)en
dc.description.provenanceApproved for entry into archive by Esra Diriarın (esradiriarin@siirt.edu.tr) on 2019-12-30T06:58:03Z (GMT) No. of bitstreams: 1 Metal chelate based site recognition of ceruloplasmin using molecularly imprinted polymer cryogel system (1).pdf: 1574877 bytes, checksum: d539d9c226f04e149f22825f3419f412 (MD5)en
dc.description.provenanceMade available in DSpace on 2019-12-30T06:58:03Z (GMT). No. of bitstreams: 1 Metal chelate based site recognition of ceruloplasmin using molecularly imprinted polymer cryogel system (1).pdf: 1574877 bytes, checksum: d539d9c226f04e149f22825f3419f412 (MD5) Previous issue date: 2020en
dc.identifier.citationDolak, I., Canpolat, G., Ersöz, A., & Say, R. (2019). Metal chelate based site recognition of ceruloplasmin using molecularly imprinted polymer/cryogel system. Separation Science and Technology, 1-10.en_US
dc.identifier.doi10.1080/01496395.2019.1577446
dc.identifier.endpage208en_US
dc.identifier.issue2en_US
dc.identifier.scopus2-s2.0-85062329061
dc.identifier.scopusqualityQ2
dc.identifier.startpage199en_US
dc.identifier.urihttps://doi.org/10.1080/01496395.2019.1577446
dc.identifier.urihttps://hdl.handle.net/20.500.12604/2565
dc.identifier.volume55en_US
dc.identifier.wosWOS:000501379700001
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorCanpolat, Gurbet
dc.language.isoenen_US
dc.publisherTaylor & Francis Groupen_US
dc.relation.ispartofSeparation Science and Technology
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/restrictedAccessen_US
dc.snmzKG_20241224
dc.subjectCeruloplasminen_US
dc.subjectNANA-imprinted cryogelen_US
dc.subjectmetal-chelate complexen_US
dc.subjectp-hema-mahen_US
dc.subjectselective separationen_US
dc.titleMetal chelate based site recognition of ceruloplasmin using molecularly imprinted polymer/cryogel systemen_US
dc.typeArticleen_US

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