Design and optimization of production parameters for boric acid crystals with the crystallization process in an MSMPR crystallizer using FBRM® and PVM® technologies

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dc.authoridKUTLUAY, SINAN/0000-0001-9493-918X
dc.authoridIZGI, Mehmet Sait/0000-0003-3685-3219
dc.authoridKutluay, Sinan/0000-0002-4987-6789
dc.authoridSAHIN, Omer/0000-0003-4575-3762
dc.contributor.authorKutluay, Sinan
dc.contributor.authorSahin, Omer
dc.contributor.authorCeyhan, A. Abdullah
dc.contributor.authorIzgi, M. Sait
dc.date.accessioned2024-12-24T19:27:21Z
dc.date.available2024-12-24T19:27:21Z
dc.date.issued2017
dc.departmentSiirt Üniversitesi
dc.description.abstractIn crystallization studies, newly developed technologies, such as Focused Beam Reflectance Measurement (FBRM) and Particle Vision and Measurement (PVM) are applied for determining on-line monitoring of a representation of the Chord Length Distribution (CLD) and observe the photographs of crystals respectively; moreover recently they are widely used. Properly installed, the FBRM ensures on-line determination of the CLD, which is statistically associated to the Crystal Size Distribution (CSD). In industrial crystallization, CSD and mean crystal size as well as external habit and internal structure are important characteristics for further use of the crystals. In this paper, the effect of residence time, stirring speed, feeding rate, supersaturation level and the polyelectrolytes such as anionic polyacrylamide (APAM) and non-ionic polyacrylamide (NPAM) on the CLD as well as the shape of boric acid crystals were investigated by using the FBRM G600 and the PVM V819 probes respectively in an MSMPR (Mixed Suspension Mixed Product Removal) crystallizer. The CSD and kinetic data were determined experimentally using continuous MSMPR crystallizer running at steady state. The population density of nuclei, the nucleation rate and the growth rate were determined from the experimental population balance distribution when the steady state was reached. (C) 2017 Published by Elsevier B.V.
dc.description.sponsorshipEti Mine Works General Management [ETI MADEN] [17/02/2014-17/01/2016]
dc.description.sponsorshipThis work was supported by Eti Mine Works General Management [ETI MADEN, project number: 17/02/2014-17/01/2016].
dc.identifier.doi10.1016/j.jcrysgro.2017.03.027
dc.identifier.endpage180
dc.identifier.issn0022-0248
dc.identifier.issn1873-5002
dc.identifier.scopus2-s2.0-85017251431
dc.identifier.scopusqualityQ2
dc.identifier.startpage172
dc.identifier.urihttps://doi.org/10.1016/j.jcrysgro.2017.03.027
dc.identifier.urihttps://hdl.handle.net/20.500.12604/6612
dc.identifier.volume467
dc.identifier.wosWOS:000401128400027
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier Science Bv
dc.relation.ispartofJournal of Crystal Growth
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241222
dc.subjectFBRM
dc.subjectPVM
dc.subjectMSMPR
dc.subjectCLD
dc.subjectCrystallization
dc.subjectBoric acid
dc.titleDesign and optimization of production parameters for boric acid crystals with the crystallization process in an MSMPR crystallizer using FBRM® and PVM® technologies
dc.typeArticle

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