Synthesis and spectral studies of macrocyclic Cu(II), Ni(II) and Co(II) complexes by template reaction of 1,4-bis(3-aminopropoxy)butane with metal(II) nitrate and salicylaldehyde derivatives

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dc.authoridIlhan, Salih/0000-0003-0779-2744
dc.authoridtemel, hamdi/0000-0001-9225-7425
dc.contributor.authorIlhan, Salih
dc.contributor.authorTemel, Hamdi
dc.date.accessioned2024-12-24T19:27:29Z
dc.date.available2024-12-24T19:27:29Z
dc.date.issued2008
dc.departmentSiirt Üniversitesi
dc.description.abstractSix new macrocyclic complexes were synthesized by template reaction of salicylaldehyde derivatives with 1,4-bis(3-aminopropoxy)butane and metal(II) nitrate. The metal to ligand ratio of the complexes was found to be 1:1. The Cu(II) complexes are proposed to be square planar and the Ni(II) and Co(II) complexes are proposed to be tetrahedral geometry. Macrocyclic complexes are 1:2 electrolytes as shown by their molar conductivities (Am) in DMF (dimethylformamide) of 10(-3) M solution. The structure of metal complexes is proposed from elemental analysis, FIR, UV-vis, magnetic Susceptibility measurements, molar conductivity measurements and mass spectra. (c) 2008 Elsevier B.V. All rights reserved.
dc.identifier.doi10.1016/j.molstruc.2008.03.016
dc.identifier.endpage166
dc.identifier.issn0022-2860
dc.identifier.issn1872-8014
dc.identifier.issue1-3
dc.identifier.scopus2-s2.0-55249120271
dc.identifier.scopusqualityQ1
dc.identifier.startpage157
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2008.03.016
dc.identifier.urihttps://hdl.handle.net/20.500.12604/6666
dc.identifier.volume891
dc.identifier.wosWOS:000261537800025
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier
dc.relation.ispartofJournal of Molecular Structure
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241222
dc.subjectMacrocyclic Schiff base
dc.subjectMacrocyclic Schiff base complex
dc.subjectSalicylaldehyde derivatives
dc.subject1,2-Bis(2-formylphenyl)ethane or
dc.subject1,3-bis(2-formylphenyl)propane
dc.titleSynthesis and spectral studies of macrocyclic Cu(II), Ni(II) and Co(II) complexes by template reaction of 1,4-bis(3-aminopropoxy)butane with metal(II) nitrate and salicylaldehyde derivatives
dc.typeArticle

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