Preparation and Characterization of Activated Carbon from Sesame Seed Shells by Microwave and Conventional Heating with Zinc Chloride Activation

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dc.authoridSAKA, Cafer/0000-0003-2534-5921
dc.authoridMohammed Sharif, Yousif/0000-0002-1207-2592
dc.contributor.authorSharif, Yousif Mohammed
dc.contributor.authorSaka, Cafer
dc.contributor.authorBaytar, Orhan
dc.contributor.authorSahin, Omer
dc.date.accessioned2024-12-24T19:28:00Z
dc.date.available2024-12-24T19:28:00Z
dc.date.issued2018
dc.departmentSiirt Üniversitesi
dc.description.abstractThe preparation of activated carbon from sesame shells as raw precursor was investigated in the study by sequentially applying microwave and conventional heating methods assisted by zinc chloride activation. The optimizisation of experimental parameters including microwave power, microwave treatment time, conventional activation time, conventional activation temperature and zinc chloride concentration ratio for the microwave and conventional heating method was performed. The characterization of the prepared activated carbon was done by thermogravimetric and differential thermal measurements, infrared spectroscopy, scanning electron microscopy and specific surface area analyses. The maximum surface area of 1254m(2)/g for the prepared activated carbon was obtained at a microwave power of 750W, a microwave treatment time of 20min, an activation time of 45min, an activation temperature of 500 degrees C and zinc chloride concentration ratio of 1:1. Methylene blue and iodine adsorption capacities for the prepared activated carbon were 103 and 1199mg/g, respectively.
dc.identifier.doi10.1080/00032719.2018.1450415
dc.identifier.endpage2744
dc.identifier.issn0003-2719
dc.identifier.issn1532-236X
dc.identifier.issue17
dc.identifier.scopus2-s2.0-85046680971
dc.identifier.scopusqualityQ2
dc.identifier.startpage2731
dc.identifier.urihttps://doi.org/10.1080/00032719.2018.1450415
dc.identifier.urihttps://hdl.handle.net/20.500.12604/6882
dc.identifier.volume51
dc.identifier.wosWOS:000443983400005
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherTaylor & Francis Inc
dc.relation.ispartofAnalytical Letters
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241222
dc.subjectInfrared spectroscopy
dc.subjectmicrowave and conventional heating
dc.subjectscanning electron microscopy
dc.subjectsesame seed shell
dc.subjectthermogravimetric analysis
dc.titlePreparation and Characterization of Activated Carbon from Sesame Seed Shells by Microwave and Conventional Heating with Zinc Chloride Activation
dc.typeArticle

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