Application of magnetized fungal solid phase extractor with Fe2O3 nanoparticle for determination and preconcentration of Co(II) and Hg(II) from natural water samples

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dc.authoridSoylak, Mustafa/0000-0002-1017-0244
dc.contributor.authorOzdemir, Sadin
dc.contributor.authorMohamedsaid, Siham Abdullah
dc.contributor.authorKilinc, Ersin
dc.contributor.authorYildirim, Aydil
dc.contributor.authorSoylak, Mustafa
dc.date.accessioned2024-12-24T19:27:29Z
dc.date.available2024-12-24T19:27:29Z
dc.date.issued2018
dc.departmentSiirt Üniversitesi
dc.description.abstractPleurolus eryngii loaded Fe2O3 magnetic nanoparticles were developed as novel magnetic solid phase bio-extractors for the preconcentrations and extractions of Co(II) and Hg(II) from real samples. The metal binding surface groups of the prepared magnetic solid phase bio-extractors were investigated by FT-IR spectrometry, SEM and EDX. Several parameters influencing the magnetic extractions and preconcentrations of Co(II) and Hg (II) were examined and optimized, including pH, flow rate, quantity of P. eryngii, quantity of Fe2O3 magnetic nanoparticle, eluent type, concentration and volume, sample volume, and foreign ions. A good reusage (35 times) was obtained with the relative standard deviation (RSD) of < 5.0% for both magnetic solid phase bio-extractors. The biosorption capacities were determined for Co(II) and Hg(II) as 25.4 mg g(-1) and 30.3 mg g(-1), respectively, using P. eryngii loaded Fe2O3 magnetic nanoparticle column. The preconcentration factors for Co(II) and Hg(II) were found as 80 and 100, respectively, when using P. eryngii loaded Fe2O3 magnetic nanoparticle column. The developed procedures were validated through analysis of the certified reference materials and successfully utilized for the determinations of Co(II) and Hg(II) in real samples by inductively coupled plasma optical emission spectrometry (ICP-OES) with satisfactory results.
dc.description.sponsorshipMersin Technology Transfer Office Academic Writing Center of Mersin University
dc.description.sponsorshipThis academic work was linguistically supported by the Mersin Technology Transfer Office Academic Writing Center of Mersin University.
dc.identifier.doi10.1016/j.microc.2018.07.032
dc.identifier.endpage204
dc.identifier.issn0026-265X
dc.identifier.issn1095-9149
dc.identifier.scopus2-s2.0-85051119776
dc.identifier.scopusqualityQ1
dc.identifier.startpage198
dc.identifier.urihttps://doi.org/10.1016/j.microc.2018.07.032
dc.identifier.urihttps://hdl.handle.net/20.500.12604/6661
dc.identifier.volume143
dc.identifier.wosWOS:000447097000026
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier Science Bv
dc.relation.ispartofMicrochemical Journal
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241222
dc.subjectPleuronis eryngii
dc.subjectCo(II) and Hg(II)
dc.subjectFe2O3 nanoparticle
dc.subjectMagnetic solid phase extraction
dc.titleApplication of magnetized fungal solid phase extractor with Fe2O3 nanoparticle for determination and preconcentration of Co(II) and Hg(II) from natural water samples
dc.typeArticle

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