Synthesis and characterisation of Schiff base macrocyclic Pb(II), Zn(II), Cd(II) and La(III) complexes by template reaction of (±)-trans-1,2-diaminocyclohexane with metal nitrates and salicylaldehyde derivatives
dc.authorid | Ilhan, Salih/0000-0003-0779-2744 | |
dc.contributor.author | Ilhan, Salih | |
dc.date.accessioned | 2024-12-24T19:31:00Z | |
dc.date.available | 2024-12-24T19:31:00Z | |
dc.date.issued | 2009 | |
dc.department | Siirt Üniversitesi | |
dc.description.abstract | Eight macrocyclic complexes have been synthesised by template reaction of (+/-)-trans-1,2-diaminocyclohexane with metal nitrates and 1,10-bis(2-formylphenyl)-1,4,7,10-tetraoxadecane or 1,7-bis(2-formylphenyl)-1,4,7-trioxaheptane, and their structures are proposed on the basis of elemental analysis, FT-IR, UV-Vis, molar conductivity measurements, H-1 The complexes NMR and mass spectra. The metal-to-ligand molar ratios are 1 : 1 in the complexes, which are 1 : 2 electrolytes for Pb(II), Cd(II) and Zn(II) and 1 : 3 electrolytes for La(III) | |
dc.identifier.doi | 10.3184/030823409X12596000099172 | |
dc.identifier.endpage | 769 | |
dc.identifier.issn | 1747-5198 | |
dc.identifier.issn | 2047-6507 | |
dc.identifier.issue | 12 | |
dc.identifier.scopus | 2-s2.0-73949084765 | |
dc.identifier.scopusquality | Q3 | |
dc.identifier.startpage | 766 | |
dc.identifier.uri | https://doi.org/10.3184/030823409X12596000099172 | |
dc.identifier.uri | https://hdl.handle.net/20.500.12604/7765 | |
dc.identifier.wos | WOS:000273946700014 | |
dc.identifier.wosquality | N/A | |
dc.indekslendigikaynak | Web of Science | |
dc.indekslendigikaynak | Scopus | |
dc.language.iso | en | |
dc.publisher | Sage Publications Ltd | |
dc.relation.ispartof | Journal of Chemical Research | |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | |
dc.rights | info:eu-repo/semantics/closedAccess | |
dc.snmz | KA_20241222 | |
dc.subject | macrocyclic Schiff base complexes | |
dc.subject | 1,7-bis(2-formylphenyl)-1,4,7-trioxaheptane | |
dc.subject | 1,10-bis(2-formylphenyl)-1,4,7,10-tetraoxadecane | |
dc.subject | (+/-)-trans-1,2-diaminocyclohexane | |
dc.title | Synthesis and characterisation of Schiff base macrocyclic Pb(II), Zn(II), Cd(II) and La(III) complexes by template reaction of (±)-trans-1,2-diaminocyclohexane with metal nitrates and salicylaldehyde derivatives | |
dc.type | Article |