Anoxybacillus sp. SO B1-Immobilized Amberlite XAD-16 for Solid-Phase Preconcentration of Cu(II) and Pb(II) and Their Determinations by Flame Atomic Absorption Spectrometry

Basit Öğe Kaydı
dc.authoridDUNDAR, ABDURRAHMAN/0000-0002-7930-1054
dc.authoridOkumus, Veysi/0000-0002-5505-2700
dc.contributor.authorOral, Elif Varhan
dc.contributor.authorOzdemir, Sadin
dc.contributor.authorDolak, Ibrahim
dc.contributor.authorOkumus, Veysi
dc.contributor.authorDundar, Abdurrahman
dc.contributor.authorZiyadanogullari, Berrin
dc.contributor.authorAksoy, Zehra
dc.date.accessioned2024-12-24T19:28:16Z
dc.date.available2024-12-24T19:28:16Z
dc.date.issued2015
dc.departmentSiirt Üniversitesi
dc.description.abstractA new method for the determination of Cu(II) and Pb(II) by flame atomic absorption spectrometry (FAAS) after preconcentrating on a column containing Anoxybacillus sp. SO B1-immobilized Amberlite XAD-16 was developed. The functional groups of Anoxybacillus sp. SO B1 immobilized on Amberlite XAD-16 were characterized in KBr tablets by Fourier transform infrared (FT-IR) spectrometry. Various parameters such as pH, amount of the adsorbent, eluent type and volume, and flow rate of the sample solution were studied. The optimum pH values of quantitative sorption for Cu(II) and Pb(II) were found to be pH 7.0 and 5.0 and Cu(II) and Pb(II) ions could be quantitatively eluted with 5.0ml of 1.0mol L-1 HCI and 10.0ml of 0.25mol L-1 HNO3, respectively. Recoveries of Cu(II) and Pb(II) were found to be 100.9 +/- 1.57% and 100.3 +/- 0.49% (N = 5), the limits of detection of Cu(II) and Pb(II) in the determination by FAAS (3s, N = 10) were found to be 0.8 and 1.6 mu g L-1, respectively. The proposed enrichment method was applied for metal ion determination from water samples such as two parts of Tigris River water in Diyarbakir and Elazig, Lake of Hazar in Elazig, and tap water in Diyarbakir. Furthermore, the accuracy of the proposed method was verified by studying the analytical recovery and by analyzing certified reference material (NCS-DC 73350 leaves of poplar).
dc.identifier.doi10.1080/10889868.2014.978837
dc.identifier.endpage150
dc.identifier.issn1088-9868
dc.identifier.issn1547-6529
dc.identifier.issue2
dc.identifier.scopus2-s2.0-84930243624
dc.identifier.scopusqualityQ2
dc.identifier.startpage139
dc.identifier.urihttps://doi.org/10.1080/10889868.2014.978837
dc.identifier.urihttps://hdl.handle.net/20.500.12604/6996
dc.identifier.volume19
dc.identifier.wosWOS:000355261100005
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherTaylor & Francis Inc
dc.relation.ispartofBioremediation Journal
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241222
dc.subjectenrichment method
dc.subjectimmobilization
dc.subjectamberlite XAD-16
dc.subjectflame atomic absorption spectrometry
dc.subjectAnoxybacillus sp. SO B1
dc.titleAnoxybacillus sp. SO B1-Immobilized Amberlite XAD-16 for Solid-Phase Preconcentration of Cu(II) and Pb(II) and Their Determinations by Flame Atomic Absorption Spectrometry
dc.typeArticle

Dosyalar

Koleksiyon

WOS İndeksli Yayınlar Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu