Synthesis of complexes of Pb(II), Cd(II), Zn(II), Ni(II), La(III) and Cu(II) with a Schiff base macrocyclic ligand containing pyridine

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dc.authoridtemel, hamdi/0000-0001-9225-7425
dc.authoridIlhan, Salih/0000-0003-0779-2744
dc.contributor.authorIlhan, Salih
dc.contributor.authorTemel, Hamdi
dc.date.accessioned2024-12-24T19:31:00Z
dc.date.available2024-12-24T19:31:00Z
dc.date.issued2010
dc.departmentSiirt Üniversitesi
dc.description.abstract1,5-bis(2-formylphenyl)pentane (synthesised from 1,5 dibromopentane and salicylaldehyde). reacts with 2,6-diaminopyridine to give a new macrocyclic ligand that gives Cu(II), Ni(II), Pb(II), Zn(II), Cd(II) and La(III) complexes by reaction with Cu(NO3)(2)center dot 3H(2)O, Ni(NO3)(2)center dot 6H(2)O, Pb(NO3)(2), Zn(NO3)(2)center dot 6H(2)O, Cd(NO3)(2)center dot 4H(2)O and La(NO3)(3)center dot 6H(2)O respectively. The ligand and its metal complexes have been characterised by elemental analysis, IR, H-1 and C-13 NMR, UV-Vis spectra, magnetic susceptibility, conductivity measurements and mass spectra. All complexes are diamagnetic and the Cu(II) complex is binuclear.
dc.identifier.doi10.3184/030823410X12744563061343
dc.identifier.endpage306
dc.identifier.issn1747-5198
dc.identifier.issn2047-6507
dc.identifier.issue6
dc.identifier.scopus2-s2.0-77956025075
dc.identifier.scopusqualityQ3
dc.identifier.startpage304
dc.identifier.urihttps://doi.org/10.3184/030823410X12744563061343
dc.identifier.urihttps://hdl.handle.net/20.500.12604/7767
dc.identifier.wosWOS:000279865700002
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSage Publications Ltd
dc.relation.ispartofJournal of Chemical Research
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_20241222
dc.subjectmacrocyclic Schiff base complexes
dc.subject1,5-bis(2-formylphenyl)pentane
dc.subject2,6-diaminopyridine
dc.titleSynthesis of complexes of Pb(II), Cd(II), Zn(II), Ni(II), La(III) and Cu(II) with a Schiff base macrocyclic ligand containing pyridine
dc.typeArticle

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