Anoxybacillus sp. SO B1 immobilized Amberlite XAD-16 for solid phase preconcentration of Cu(II), Pb(II) and their determinations by flame atomic absorption spectrometry

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dc.authoridhttps://orcid.org/0000-0002-5505-2700en_US
dc.contributor.authorVarhan, Elif
dc.contributor.authorÖzdemir, Sadin
dc.contributor.authorDolak, İbrahim
dc.contributor.authorOkumuş, Veysi
dc.contributor.authorDündar, Abdurrahman
dc.contributor.authorZiyadanoğulları, Berrin
dc.contributor.authorAksoy, Zehra
dc.contributor.authorOnat, Ruken
dc.date.accessioned2019-12-23T10:53:26Z
dc.date.available2019-12-23T10:53:26Z
dc.date.issued2016en_US
dc.departmentFen - Edebiyat Fakültesien_US
dc.description.abstractA new method for the determination of Cu(II) and Pb(II) by flame atomic absorption spectrometry (FAAS) after preconcentrating on a column containing Anoxybacillus sp. SO B1–immobilized Amberlite XAD-16 was developed. The functional groups of Anoxybacillus sp. SO B1 immobilized on Amberlite XAD-16 were characterized in KBr tablets by Fourier transform infrared (FT-IR) spectrometry. Various parameters such as pH, amount of the adsorbent, eluent type and volume, and flow rate of the sample solution were studied. The optimum pH values of quantitative sorption for Cu(II) and Pb(II) were found to be pH 7.0 and 5.0 and Cu(II) and Pb(II) ions could be quantitatively eluted with 5.0 ml of 1.0 mol L¡1 HCI and 10.0 ml of 0.25 mol L¡1 HNO3, respectively. Recoveries of Cu(II) and Pb(II) were found to be 100.9 § 1.57% and 100.3 § 0.49% (N D 5), the limits of detection of Cu(II) and Pb(II) in the determination by FAAS (3 s, N D 10) were found to be 0.8 and 1.6 mg L¡1, respectively. The proposed enrichment method was applied for metal ion determination from water samples such as two parts of Tigris River water in Diyarbakır and Elazı_g, Lake of Hazar in Elazı_g, and tap water in Diyarbakır. Furthermore, the accuracy of the proposed method was verified by studying the analytical recovery and by analyzing certified reference material (NCS-DC 73350 leaves of poplar).en_US
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dc.description.provenanceMade available in DSpace on 2019-12-23T10:53:26Z (GMT). No. of bitstreams: 1 A26.pdf: 289046 bytes, checksum: d46af9778e533bb845502ad3e91133c2 (MD5) Previous issue date: 2016en
dc.identifier.citationOral, Elif Varhan, et al. "Anoxybacillus sp. SO B1–immobilized Amberlite XAD-16 for solid-phase preconcentration of Cu (II) and Pb (II) and their determinations by flame atomic absorption spectrometry." Bioremediation Journal 19.2 (2015): 139-150.en_US
dc.identifier.endpage150en_US
dc.identifier.issue2en_US
dc.identifier.startpage139en_US
dc.identifier.urihttps://hdl.handle.net/20.500.12604/2363
dc.identifier.volume19en_US
dc.institutionauthorOkumuş, Veysi
dc.language.isoenen_US
dc.publisherBioremediation Journalen_US
dc.relation.ispartofBioremediation Journal
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.snmz#KayıtKontrol#
dc.subjectamberlite XAD-16en_US
dc.subjectAnoxybacillus sp. SO B1en_US
dc.subjectEnrichment methoden_US
dc.subjectflame atomic absorption spectrometryen_US
dc.subjectimmobilizationen_US
dc.titleAnoxybacillus sp. SO B1 immobilized Amberlite XAD-16 for solid phase preconcentration of Cu(II), Pb(II) and their determinations by flame atomic absorption spectrometryen_US
dc.typeArticleen_US

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